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In this study, cobalt oxide (Co3O4) was prepared by thermolysis of cobalt (II) oxalate at ???????????? This oxide was characterized by IR spectroscopy, XRD (X-ray diffraction) and SEM (scanning electron microscopy). The adsorption of phenol and lead (II) ions, both singly and in combination, by obtained and characterized Co3O4 was studied in batch system. Kinetic and equilibrium experiments were conducted to study the effects of solid : liquid ratio, pH, contact time and initial concentration of the pollutants. Th...

The purpose of the study was to develop an electrochemical method for detection of lead at low level of contamination in water samples using a carbon glassy electrode modified with the functionalized azulene: (2E)-2-(azulen-1-ylmethylidene) hydrazine carbothioamide (L) as a complexing polymer film. The modified electrodes were prepared in L solutions (1mM) in acetonitrile (CH3CN) containing tetra n-butyl ammonium perchlorate (0.1 M TBAP) as supporting electrolyte. The analyses were performed on Autolab PGSTAT 12 P...

To study the process of refining of crude antimony containing as hard-to-remove admixtures of lead and tin, thermal studies of model and experimental samples of antimony were carried out. As a refining reagent, a melt prepared from sodium dihydrogen phosphate and orthophosphoric acid was used. The results of the study showed that the lead oxide after the process of dehydration and dehydration of sodium phosphate salts at 760 °C interacts with the decomposition product of the refining reagent to form stable phospho...