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N-METHYL-D-GLUCOSE AMINE SYNTHESIS OVER NI BASED CATALYSTS
(STEF92 Technology, 2020-09-20, Степан Петрович Михайлов, Mikhail G. Sulman, Valentina G. Matveeva, А. И. Сидоров, Valentin Yu. Doluda)
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N-methyl-D-glucose amine is an amine formed by reduction of glucosylamine or glucose oxime. N-alkylated glucamines are prepared from D-glucose and relevant alkylamines. Here synthesis of N-methyl-D-glucose amine by consecutive condensation of D-glucose with methylamine in ethanol media followed by reduction over Ni containing hyper crosslinked polystyrene is reported. In typical synthesis 50 g sample of D-glucose monohydrate was added to 150 ml of ethanol (96 wt.%) and stirred under 600 rpm for 30 minutes. Suspens...
Ecology and Environmental Protection2020