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The growing demand for refractory rare metals, such as niobium, necessitates the development of efficient extraction methods from alternative sources, including industrial waste from metallurgical plants enriched with niobium and zirconium. This study investigates the solvent extraction of niobium from a fluoride-sulfuric acid solution obtained by leaching rare-metal-containing waste from titanium-magnesium production. The efficiency of niobium recovery using a trialkyl phosphine oxide-based extractant (Cyanex 923...