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This paper presents the geochemical forms of arsenic that are present in bottom sediments of rivers and surface waters under various oxidative conditions. In summer, in the rivers with the high anthropogenic load the redox potential of bottom sediments varies from 78 mV to 255 mV (at a temperature of 16-20?C), which corresponds to oxidative and mixed oxidative-reductive conditions. It is shown that under these conditions arsenic is present in the form of insoluble arsenous acid, partially ionized arsenic acid and ...