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Technology of self-propagating high-temperature synthesis (SHS) is used to obtain ligature in Fe-B system. The SHS Technology can also be successfully used for obtaining ligatures from metallurgical waste, which is the subject of investigation in the presented paper. To separate melted alloy of Fe-B and slag of the process, synthesis is carried out in centrifugal machine. Separation degree between melted alloy of Fe-B and slag in the graphite cup inside the rotating reactor, and, therefore, output degree of final ...