ULTRASONIC EXTRACTION OF FRUCTANS FROM THE TUBERS OF JERUSALEM ARTICHOKE: OPTIMIZATION OF CONDITIONS, PURIFICATION METHODS, C-13NMR SPECTROSCOPY OF THE PRODUCT

Wack M., Blaschek W. Determination of the structure and degree of polymerisation of fructans from Echinacea purpurea roots//Carbohydrate Research. 2006. V. 341. № 9. P. 1147–1153

Gibson G., Roberfroid M.B. Dietary modulation of the human colonic microflora – introducing the concept of prebiotics//J. Nutr. 1995. V. 125. P. 1402–1412

Su P., Henriksson1 A., Mitchell H . Prebiotics enhance survival and prolong the retention period of specific probiotic inocula in an in vivo murine model//Journal of Applied Microbiology. 2007. V. 103. P. 2392–2400

Rossi M., Corradini C., Amaretti A., Nicolini M., Pompei A., Zanoni S., Matteuzzi D. Fermentation of Fructooligosaccharides and Inulin by Bifidobacteria: a Comparative Study of Pure and Fecal Cultures// J. of Applied and Environmental Microbiology. 2005, V. 71, № 10, P. 6150–6158

Makras L., Van Acker G., De Vuyst L . Lactobacillus paracasei subsp. paracasei 8700:2 Degrades Inulin-Type Fructans Exhibiting Different Degrees of Polymerization// J. of Applied and Environmental Microbiology. 2005, V. 71. № 11. P. 6531–

Wei, L., Wang, J., Zheng, X., Teng, D., Yang, Y., Cai, C., Feng, T., Zhang, F. Studies on the extracting technical conditions of inulin from Jerusalem artichoke tubers //Journal of Food Engineering. Vol. 79, № 3, 2007, P. 1087–1093

Lopez-Molina D., Na varro-Martınez M.D., Melgarejo F. R., Hiner A.N.P., Chazarra S., Rodrıguez -Lopez J. N . Molecular properties and prebiotic effect of inulin obtained from artichoke (Cynara scolymus L.)//Phytochemistry. 2005. V. 66. № 12. P. 1476–

Gomez E., Tuohy K.M., Gibson G.R., Klinder A., Costabile A . In vitro evaluation of the fermentation properties and potential prebiotic activity of Agave fructans// Journal of Applied Microbiology. 2010. V. 108. P. 2114–

Kelly G. Inulin-type prebiotics – a review: Part 1. Altern. Med. Rev. 2008. V. 13. P. 315–329

Lia W., Zhangb J., Yub C., Lia Q., Donga F., Wanga G., Gud G., Guo Z.. Extraction, degree of polymerization determination and prebiotic effect evaluation of inulin from Jerusalem artichoke. Carbohydr Polym. 2015. V. 5. № 121. Р. 315-

Golubev V. N., Volkova I. V., Kushalakov H.M. Jerusalem artichoke. Composition, properties, processing methods, applications. (in Russian) – Astrakhan: Publishing and Printing Complex "Volga", 1995. – P. 81-89.

Shakir I., Panfilov V., Kulinenkov D., Manakov M. Inulin recerving during Jerusalem Artichoke complex processing // ISEB-99 Meeting Biopolimers, 2- 5.03.1999, Leipzig, Germany. P. 38-39. International Multidisciplinary Scientific GeoConfenferences SGEM 2015 www.sgem.org 15th International Multidisciplinary Scientific GeoConferences SGEM2015

Chen R., Li Y., Dong H., Liu Z., Li S., Yang S., Li X. Optimization of ultrasonic extraction process of polysaccharides from Ornithogalum Caudatum Ait and evaluation of its biological activities. Ultrason Sonochem, 2012, vol. 19/ issue 6, pp 1160-1168

Ebringerova A., Hromadkova Z . Effect of ultrasound on the extractibility of corn bran hemicelluloses. //Ultrasonics Sonochemistry. 2002. V. 9. P. 225–229.

Cerantola S., Kervarec N., Pichon R., Magne C., Bessieresa M.-A., Deslandes E. NMR characterisation of inulin-type fructooligosaccharides as the major wat er- soluble carbohydrates from Matricaria maritima (L.).// Carbohydrate Research. 2004. V. 339. P. 2445–2449. International Multidisciplinary Scientific GeoConfenferences SGEM 2015 www.sgem.org

Wack M., Blaschek W. Determination of the structure and degree of polymerisation of fructans from Echinacea purpurea roots//Carbohydrate Research. 2006. V. 341. № 9. P. 1147–1153

Gibson G., Roberfroid M.B. Dietary modulation of the human colonic microflora – introducing the concept of prebiotics//J. Nutr. 1995. V. 125. P. 1402–1412

Su P., Henriksson1 A., Mitchell H . Prebiotics enhance survival and prolong the retention period of specific probiotic inocula in an in vivo murine model//Journal of Applied Microbiology. 2007. V. 103. P. 2392–2400

Rossi M., Corradini C., Amaretti A., Nicolini M., Pompei A., Zanoni S., Matteuzzi D. Fermentation of Fructooligosaccharides and Inulin by Bifidobacteria: a Comparative Study of Pure and Fecal Cultures// J. of Applied and Environmental Microbiology. 2005, V. 71, № 10, P. 6150–6158

Makras L., Van Acker G., De Vuyst L . Lactobacillus paracasei subsp. paracasei 8700:2 Degrades Inulin-Type Fructans Exhibiting Different Degrees of Polymerization// J. of Applied and Environmental Microbiology. 2005, V. 71. № 11. P. 6531–

Wei, L., Wang, J., Zheng, X., Teng, D., Yang, Y., Cai, C., Feng, T., Zhang, F. Studies on the extracting technical conditions of inulin from Jerusalem artichoke tubers //Journal of Food Engineering. Vol. 79, № 3, 2007, P. 1087–1093

Lopez-Molina D., Na varro-Martınez M.D., Melgarejo F. R., Hiner A.N.P., Chazarra S., Rodrıguez -Lopez J. N . Molecular properties and prebiotic effect of inulin obtained from artichoke (Cynara scolymus L.)//Phytochemistry. 2005. V. 66. № 12. P. 1476–

Gomez E., Tuohy K.M., Gibson G.R., Klinder A., Costabile A . In vitro evaluation of the fermentation properties and potential prebiotic activity of Agave fructans// Journal of Applied Microbiology. 2010. V. 108. P. 2114–

Kelly G. Inulin-type prebiotics – a review: Part 1. Altern. Med. Rev. 2008. V. 13. P. 315–329

Lia W., Zhangb J., Yub C., Lia Q., Donga F., Wanga G., Gud G., Guo Z.. Extraction, degree of polymerization determination and prebiotic effect evaluation of inulin from Jerusalem artichoke. Carbohydr Polym. 2015. V. 5. № 121. Р. 315-

Golubev V. N., Volkova I. V., Kushalakov H.M. Jerusalem artichoke. Composition, properties, processing methods, applications. (in Russian) – Astrakhan: Publishing and Printing Complex "Volga", 1995. – P. 81-89.

Shakir I., Panfilov V., Kulinenkov D., Manakov M. Inulin recerving during Jerusalem Artichoke complex processing // ISEB-99 Meeting Biopolimers, 2- 5.03.1999, Leipzig, Germany. P. 38-39. International Multidisciplinary Scientific GeoConfenferences SGEM 2015 www.sgem.org 15th International Multidisciplinary Scientific GeoConferences SGEM2015

Chen R., Li Y., Dong H., Liu Z., Li S., Yang S., Li X. Optimization of ultrasonic extraction process of polysaccharides from Ornithogalum Caudatum Ait and evaluation of its biological activities. Ultrason Sonochem, 2012, vol. 19/ issue 6, pp 1160-1168

Ebringerova A., Hromadkova Z . Effect of ultrasound on the extractibility of corn bran hemicelluloses. //Ultrasonics Sonochemistry. 2002. V. 9. P. 225–229.

Cerantola S., Kervarec N., Pichon R., Magne C., Bessieresa M.-A., Deslandes E. NMR characterisation of inulin-type fructooligosaccharides as the major wat er- soluble carbohydrates from Matricaria maritima (L.).// Carbohydrate Research. 2004. V. 339. P. 2445–2449. International Multidisciplinary Scientific GeoConfenferences SGEM 2015 www.sgem.org