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NON-DESTRUCTIVE RESEARCH OF CEMENT COMPOSITE DEGRADATION USING X-RAY CT

Vendula Zajícová

First published: 2019-06-20https://doi.org/10.5593/sgem2019/1.2/s02.049View metrics

Abstract

The paper describes the use of methods of visualization and non-destructive investigation of spatial distribution of changes in the structure of the monitored material, which was a cement composite with admixture of blast furnace slag. The test specimens in the shape of the cylinders with a diameter of 24mm and a height of 25mm were placed in an aggressive sulfate environment represented by bacteria of the microorganism Acidithiobacillus thiooxidans for 6 months. To investigate the spatial distribution and the degree of degradation of the affected area, the X-ray computed tomography (CT) method by Nikon XT H 225 ST industrial X-ray system scanner was used. The results were analyzed by VG Studio Max 3.2 software. Comparing the reference 3D images before and after the degradation tests has shown an aggressive microbacterial environment. The visible corrosion of the cement filling reaches a depth of approx. 3.5mm. At the same time, image analysis showed a remarkable transfer of material from the corrosion area to the outer and inner free surfaces of the sample. The precipitated material on the surfaces partially increased the geometric dimensions of the sample and caused partial ingrown of the communicative pores in the concete specimens. The analysis of the change in the density distribution of the material shows the ingrown of some pores in the material and indicates a change in the representation of individual density phases. This demonstrates the corrosion degradation of the material composition.

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Publication details

Title
NON-DESTRUCTIVE RESEARCH OF CEMENT COMPOSITE DEGRADATION USING X-RAY CT
Authors
Vendula Zajícová
Proceedings
SGEM International Multidisciplinary Scientific GeoConference EXPO Proceedings; 19th SGEM International Multidisciplinary Scientific GeoConference EXPO Proceedings19th, Science and Technologies in Geology, Exploration And Mining
Publisher
STEF92 Technology
Year
2019
Pages
385-392
SWS Citekey
Zajicova20192385392
ISSN
1314-2704
ISBN
978-619-7408-77-5
Language
en
Publication type
Conference Paper
Keywords
References6
  1. Zajicova V, Stas L, Soucek K and Georgiovska L, Visualization of pore space in the granitic rocks using x-ray computed tomography 2016 16th Int. Mul. Sci. Geo. SGEM 2016(Albena) vol 3 (Sofia: STEF92 Technology Ltd.) pp 355-362.

  2. Stas L, Zajicova V, Georgiovska L, Soucek K, Visualization of pore space in the rocks. In Tomach, P. (ed.), Nowoczesne metody eksploatacji węgla i skał zwięzłych. Monografia, pp 44-51, 2015

  3. Kak A. C., Slaney M., Principles of Computerized Tomographic Imaging, Society of Industrial and Applied Mathematics, 2001.

  4. Tullborg, E.-L., Larson, S.Å. (2006). Porosity in crystalline rocks – A matter of scale. Engineering Geology 84, 75–83.

  5. Smolakova M, Estokova A, Vaclavik V, Soucek K and Zajicova V, Determination of durability of mortar with slag exposed to bacterial environment, 2018 IOP Conf. Ser.: Mater. Sci. Eng. 385 012052

  6. Bossa N, Chaurand P, Vicente J, Borschneck D, Levard C, Aguerre-Chariol O and Rose J 2015, Cem. Concr. Res. 67 138-147

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