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Electrochemical method for the preparation of high-quality nanostructured surfaces and functionalization through active biomolecules electrodepositions are highlighted in this work. There are two applied electrochemical methods in order to obtain hybrid and nanocomposite structured layers or advanced functionalization of material surfaces: (i) electrochemical oxidation or anodization of materials resulting nanoporous or nanostructured oxide films and (ii) direct electrochemical synthesis by electrocodeposition pro...