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In the world, over 18 million vehicles are rejected annually from operation. The spent catalysts are obtained from th e vehicles at the end of their life cycle as well as the vehicles which do not meet the prescribed st andards in the ECO test respected to the composition of exhaust gases. The basis of each catalyst is a ceramic monolith with deposited valuable platinum metals. The spent catalysts are solid waste and also the rich raw material for recovery of precious metals. The aim of this paper is a separation ...