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The results of methane and total hydrogen sulphide detection in bottom sediments of small rivers as well as fresh and slightly saline water bodies of the Eastern Donbass are presented. The content of CH4 in sediments of water bodies of Eastern Donbass varies between 0.04-26.8 ?g/g wet mass (w.m.), ?H2S content varies from to less 0.005 than 4.02 mg/g w.m. The maximum concentrations of methane were recorded in the bottom sediments of the Glubokaya River (Station No. 7), while the maximum of the content ?H2S is conf...