Publication
STUDY OF TIN SELENIDE MECHANOCHEMICAL SYNTHESIS
(Stef92 Technology, 2011-06-20, Marcela Achimovičová)
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Tin selenide SnSe was synthesized from tin and selenium powder precursors by high- energy milling in pl anetary ball mill. X-ray diffractio n analysis confirmed that an orthorhombic tin selenide SnSe phase was formed already after 4 min of milling. 119Sn Mössbauer spectroscopy documented the values of SnSe isomer shifts corresponded to Sn in the oxidation state II. The size and morphology of tin selenide particles were studied by specific surface area measuremen ts, and transmission electron microscopy. Specific ...
Micro and Nano Technologies2011