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The article presents the study on the effect of thermal and acidic hydrolysis treatment on the antioxidant activity of humic acids. It clarifies the changes in macromolecule structure resulted from the variations in periphery/nucleus ratio. Using the differential-thermal analysis, kinetic parameters of humic acid thermal-oxidative destruction were determined. The studied samples of humic acids were divided into three groups: humic acids extracted from air-dried fen and terrestrial fuscum peat, humic acids subjecte...