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Gypsum composites are promising building materials, but they have disadvantages such as low strength and water resistance. To improve these properties, a self-reinforcement method can be used, where the gypsum matrix is reinforced with crystals other than gypsum. One type of such crystals is ettringite. To obtain a self-reinforced gypsum composite, it is necessary to maintain a high pH environment and sufficient ions to form ettringite. In this work high-calcium fly ash, which is a waste product of coal combustion...